allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Base Information

Chemical Name:allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside
CAS No.:1356821-78-7
Molecular Formula:C₂₈H₃₀ClN₃O₄S
Molecular Weight:540.083
Hs Code.:

Synonyms:allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Suppliers and Price of allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

There total 6 articles about allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1356821-77-6
allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thionyl)-1,2,4-triazolin-4-yl]-β-D-ribofuranoside

: 1356821-78-7
allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 17h;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: 1356821-74-3
allyl 2,3-O-cyclopentylidene-5-deoxy-5-isothiocyanate-β-D-ribofuranoside

: 1356821-78-7
allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1,4-dioxane / 24 h / 20 °C / Inert atmosphere

2: sodium ethanolate / ethanol / 24 h / Reflux

3: acetic acid / 24 h / 40 °C

4: potassium carbonate / acetone / 17 h / 20 °C

With sodium ethanolate; potassium carbonate; acetic acid; In 1,4-dioxane; ethanol; acetone;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: allyl 2,3-O-cyclopentylidene-β-D-ribofuranoside

: 1356821-78-7
allyl 5-deoxy-5-[(5-p-chlorophenyl-3-thiobenzyl)-1,2,4-triazol-4-yl]-2,3-O-cyclopentylidene-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere

3: triphenylphosphine / 1,4-dioxane / 24 h / 20 °C / Inert atmosphere

4: 1,4-dioxane / 24 h / 20 °C / Inert atmosphere

5: sodium ethanolate / ethanol / 24 h / Reflux

6: acetic acid / 24 h / 40 °C

7: potassium carbonate / acetone / 17 h / 20 °C

With pyridine; sodium azide; sodium ethanolate; potassium carbonate; acetic acid; triphenylphosphine; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2011.10.028