N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

Base Information

Chemical Name:N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine
CAS No.:78217-89-7
Molecular Formula:C₃₀H₃₄N₄O₁₀
Molecular Weight:610.621
Hs Code.:

N<sup>4</sup>-<N-(2,3-dihydroxybenzoyl)glycyl>-N<sup>1</sup>,N<sup>8</sup>-bis(2,3-dihydroxybenzoyl)spermidine

Synonyms:N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

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Chemical Property of N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

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Technology Process of N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

There total 17 articles about N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 78217-86-4
N⁴--N¹,N⁸-bis(2,3-dimethoxybenzoyl)spermidine

: 78217-89-7
N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

Guidance literature:: With boron tribromide; In dichloromethane; for 20h; 0 deg C to room temperature;
DOI:10.1021/jo00335a041

Reference yield: 75.0%

: 114482-48-3
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)butyl>-N-2,3-dibenzyloxybenzoylglycylamide

: 78217-89-7
N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

Guidance literature:: With palladium hydroxide - carbon; In ethanol; cyclohexene; for 3h; Heating;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 1216-04-2
N-(2-Cyanoethyl)-N-(3-cyanopropyl)-benzylamine

: 78217-89-7
N⁴--N¹,N⁸-bis(2,3-dihydroxybenzoyl)spermidine

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / LiAlH₄, AlCl₃

2: 98 percent / triethylamine / CH₂Cl₂ / 18 h / 0 deg C to room temperature

3: 98 percent / 1) H₂, 2) NaOMe / 1) PdCl₂ / 1) glacial acetic acid, room temperature, 2) MeOH, 30 min

4: 80 percent / dicyclohexylcarbodiimide, NEt₃ / CH₂Cl₂ / 48 h

5: 94 percent / BBr₃ / CH₂Cl₂ / 20 h / 0 deg C to room temperature

With lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium methylate; boron tribromide; triethylamine; dicyclohexyl-carbodiimide; palladium dichloride; In dichloromethane;
DOI:10.1021/jo00335a041