1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

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Chemical Name:1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane
CAS No.:304863-05-6
Molecular Formula:C₃₅H₅₁N₃O₆S₃
Molecular Weight:706.004
Hs Code.:

Synonyms:1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

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Chemical Property of 1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

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Technology Process of 1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

There total 6 articles about 1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 742686-12-0
1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

: 304863-05-6
1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/0968-0896(96)00072-7

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 304863-05-6
1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 10percent NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

2: H₂N-NH₂ / methanol / 17 h / 50 °C

3: 77 percent / 10percent NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium hydroxide; hydrazine; In methanol; dichloromethane;
DOI:10.1016/0968-0896(96)00072-7

Reference yield:

: 151915-06-9
1-phthalimido-4-(N-benzyl)-7-<<(2-mesitylene)sulfonyl>amino>-4-azaheptane

: 304863-05-6
1-[N-(2-mesitylene)sulfonyl]amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, a) 0 deg C, 30 min, b) RT, 45 min

2: 60 percent / H₂ / methanol; ethanol / 48 h / 2585.7 Torr / Ambient temperature

3: 79 percent / 10percent NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

4: H₂N-NH₂ / methanol / 17 h / 50 °C

5: 77 percent / 10percent NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium hydroxide; hydrogen; sodium hydride; hydrazine; In methanol; ethanol; dichloromethane;
DOI:10.1016/0968-0896(96)00072-7