1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Base Information

Chemical Name:1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane
CAS No.:742686-12-0
Molecular Formula:C₂₆H₄₁N₃O₄S₂
Molecular Weight:523.761
Hs Code.:

Synonyms:1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

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Chemical Property of 1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

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Technology Process of 1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

There total 13 articles about 1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1241383-34-5
C₃₁H₄₉N₃O₆S₂

: 742686-12-0
1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1007/s11095-010-0197-4

Reference yield:

: 1-phthalimido-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

: 742686-12-0
1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: With hydrazine; In methanol; at 50 ℃; for 17h;
DOI:10.1016/0968-0896(96)00072-7

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 742686-12-0
1-amino-4-[N-(2-mesitylene)sulfonyl]-7-{N-ethyl-N-[(2-mesitylene)sulfonyl]}amino-4-azaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 10percent NaOH / CH₂Cl₂ / 3 h / 0 - 20 °C

2: H₂N-NH₂ / methanol / 17 h / 50 °C

With sodium hydroxide; hydrazine; In methanol; dichloromethane;
DOI:10.1016/0968-0896(96)00072-7