C₁₄H₁₅NO₃S

Base Information

Chemical Name:C₁₄H₁₅NO₃S
CAS No.:1421747-02-5
Molecular Formula:C₁₄H₁₅NO₃S
Molecular Weight:277.344
Hs Code.:

C<sub>14</sub>H<sub>15</sub>NO<sub>3</sub>S

Synonyms:C₁₄H₁₅NO₃S

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Chemical Property of C₁₄H₁₅NO₃S

Chemical Property:

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Technology Process of C₁₄H₁₅NO₃S

There total 3 articles about C₁₄H₁₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3678-62-4
2-chloro-4-picoline

: 918328-09-3
2-(4-methoxy-3-(methylsulfonyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1421747-02-5
C₁₄H₁₅NO₃S

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In ethanol; toluene; at 90 ℃; for 7h;

Reference yield:

: 23095-05-8
5-bromo-2-methoxybenzenesulfonyl chloride

: 1421747-02-5
C₁₄H₁₅NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; sodium sulfite / water / 22 h / 20 - 80 °C

1.2: 8 h / 120 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 8 h / 90 °C / Inert atmosphere

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / toluene; ethanol / 7 h / 90 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium hydrogencarbonate; caesium carbonate; sodium sulfite; In 1,4-dioxane; ethanol; water; toluene;

Reference yield:

: 90531-99-0
4-bromo-1-methoxy-2-(methylsulfonyl)benzene

: 1421747-02-5
C₁₄H₁₅NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 8 h / 90 °C / Inert atmosphere

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / toluene; ethanol / 7 h / 90 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; caesium carbonate; In 1,4-dioxane; ethanol; toluene;