(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

Base Information

Chemical Name:(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt
CAS No.:1348410-84-3
Molecular Formula:C₃₂H₂₈NO₅*K
Molecular Weight:545.676
Hs Code.:

Synonyms:(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

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Chemical Property of (S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

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Technology Process of (S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

There total 5 articles about (S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1316755-16-4
PD 126055

: 1348410-84-3
(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

Guidance literature:: With potassium hydroxide; In isopropyl alcohol; at 5 - 50 ℃; for 5.5h; Product distribution / selectivity;

Reference yield:

: 1871-76-7
diphenylacetic acid chloride

: 1348410-84-3
(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane; pyridine / dichloromethane / 0.33 h / -12 - -10 °C / Inert atmosphere

1.2: 0.25 h / -12 - -10 °C

2.1: hydrogenchloride / ethyl acetate; water

3.1: potassium hydroxide / isopropyl alcohol / 5.5 h / 5 - 50 °C

With pyridine; hydrogenchloride; chloro-trimethyl-silane; potassium hydroxide; In dichloromethane; water; ethyl acetate; isopropyl alcohol;

Reference yield:

: 551909-81-0
2,2-diphenyl-1-(1H-pyrazol-1-yl)ethan-1-one

: 1348410-84-3
(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, potassium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N,N',N'-tetramethylguanidine / N,N-dimethyl-formamide / 1 h / Inert atmosphere

1.2: 16 h

2.1: hydrogenchloride / ethyl acetate; water

3.1: potassium hydroxide / isopropyl alcohol / 5.5 h / 5 - 50 °C

With hydrogenchloride; potassium hydroxide; N,N,N',N'-tetramethylguanidine; In water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;