H-ALA-D-GLU-NH2

Base Information

• Chemical Name: H-ALA-D-GLU-NH2
• CAS No.: 45159-25-9
• Molecular Formula: C₈H₁₅N₃O₄
• Molecular Weight: 217.225
• Hs Code.: 2924199090
• Mol file: 45159-25-9.mol

Synonyms:D-a-Glutamine, N2-L-alanyl-;Desmuramyldipeptide; L-Alanyl-D-isoglutamine

Chemical Property of H-ALA-D-GLU-NH2

Chemical Property:

• PSA: 135.51000
• LogP: -0.04000
• Storage Temp.: -15°C

Purity/Quality:

>98% ^*data from raw suppliers

H-Ala-D-Glu-NH2 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of H-ALA-D-GLU-NH2

There total 12 articles about H-ALA-D-GLU-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

benzyloxycarbonylalanyl-D-isoglutamine (17097-05-1) → L-alanyl-D-isoglutamine (45159-25-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

Reference yield: 39.0%

(S)-1-(((R)-1-amino-5-(benzyloxy)-1,5-dioxopentan-2-yl)amino)-1-oxopropan-2-aminium 2,2,2-trifluoroacetate (66025-93-2) → L-alanyl-D-isoglutamine (45159-25-9)

Guidance literature:

(S)-1-(((R)-1-amino-5-(benzyloxy)-1,5-dioxopentan-2-yl)amino)-1-oxopropan-2-aminium 2,2,2-trifluoroacetate; With N-ethylmorpholine;; In 1,4-dioxane;

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 24h; under 1551.49 Torr;

DOI:10.1007/s11224-018-1234-x

Reference yield:

muramyl dipeptide (56772-92-0,56816-15-0,74311-89-0,80953-11-3,87420-46-0,87420-47-1,87420-48-2,87420-49-3,87420-50-6,87420-93-7,53678-77-6) → (R)-2-(((3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanoic acid (1856-93-5,13057-99-3,14468-69-0,24909-43-1,24909-48-6,61633-75-8,61665-31-4) + L-alanyl-D-isoglutamine (45159-25-9)

Guidance literature:

With apo form of the N-acetylmuramyl-L-alanine amidase from Mycobacterium abscessus; at 37 ℃; for 0.5h;

DOI:10.3390/cells9112410

upstream raw materials:

benzyloxycarbonylalanyl-D-isoglutamine

N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-isomuramyl-L-alanyl-D-isoglutamine benzyl ester

benzyl (R)-5-amino-4-((tert-butoxycarbonyl)amino)-5-oxopentanoate

tert-butoxycarbonyl-L-alanyl-D-isoglutamine benzyl ester

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