ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Base Information

Chemical Name:ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate
CAS No.:1308255-32-4
Molecular Formula:C₁₇H₂₀BN₃O₆S
Molecular Weight:405.239
Hs Code.:

Synonyms:ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

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Chemical Property of ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

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Technology Process of ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

There total 5 articles about ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1308254-86-5
4-amino-2-(aminomethyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

: 541-41-3
chloroformic acid ethyl ester

: 1308255-32-4
ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at -20 - 20 ℃; for 2h;

Reference yield:

: 16588-02-6
4-chloro-3-cyanonitrobenzene

: 1308255-32-4
ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 20 °C

2: acetic acid; chlorine / water / 2 h / 15 °C

3: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

4: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

5: triethylamine / tetrahydrofuran / 2 h / -20 - 20 °C

With 4-methyl-morpholine; ammonium hydroxide; hydrogen; chlorine; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; water; acetonitrile;

Reference yield:

: 175135-67-8
2-(benzylthio)-5-nitrobenzonitrile

: 1308255-32-4
ethyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; chlorine / water / 2 h / 15 °C

2: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

3: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

4: triethylamine / tetrahydrofuran / 2 h / -20 - 20 °C

With 4-methyl-morpholine; ammonium hydroxide; hydrogen; chlorine; acetic acid; triethylamine; In tetrahydrofuran; methanol; water; acetonitrile;