ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

Base Information

Chemical Name:ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate
CAS No.:710326-96-8
Molecular Formula:C₂₄H₃₁NO₆
Molecular Weight:429.513
Hs Code.:

Synonyms:ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

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Chemical Property of ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

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Technology Process of ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

There total 4 articles about ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 197299-09-5
3-(4-hydroxyphenyl)-2-phenylpropionic acid ethyl ester

: 710326-96-8
ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; for 17h;
DOI:10.1016/j.bmc.2004.01.048

Reference yield:

: 62517-34-4
ethyl 2-hydroxy-3-(4-hydroxyphenyl)propionate

: 710326-96-8
ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / K₂CO₃ / dimethylformamide / 4 h / 60 °C

2: 57 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 16 h / 20 °C

3: 96 percent / H₂ / Pd/C / ethanol / 2 h / 50 °C

4: 96 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 17 h / 0 - 20 °C

With hydrogen; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; toluene; 2: Mitsunobu reaction / 4: Mitsunobu reaction;
DOI:10.1016/j.bmc.2004.01.048

Reference yield:

: 141109-83-3
ethyl 3-(4-benzyloxyphenyl)lactate

: 710326-96-8
ethyl 3-[4-(2-tert-butoxycarbonylaminoethoxy)phenyl]-2-phenoxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 16 h / 20 °C

2: 96 percent / H₂ / Pd/C / ethanol / 2 h / 50 °C

3: 96 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 17 h / 0 - 20 °C

With hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In ethanol; toluene; 1: Mitsunobu reaction / 3: Mitsunobu reaction;
DOI:10.1016/j.bmc.2004.01.048