4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

Base Information

Chemical Name:4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate
CAS No.:1354818-89-5
Molecular Formula:C₂HF₃O₂*C₁₉H₁₃Cl₂N₅O₃S₂
Molecular Weight:608.406
Hs Code.:

Synonyms:4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

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Chemical Property of 4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

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Technology Process of 4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

There total 4 articles about 4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354819-10-5
C₂₈H₂₃Cl₂N₅O₅S₂

: 76-05-1
trifluoroacetic acid

: 1354818-89-5
4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 19798-80-2
2-Amino-4-chloropyridine

: 1354818-89-5
4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 4 h / 90 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 65 °C

3: dichloromethane / 1 h / 20 °C

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 89488-25-5
(5‐chloro‐2‐hydroxyphenyl)boronic acid

: 1354818-89-5
4-[2-(2-aminopyridin-4-yl)-4-chlorophenoxy]-3-chloro-N-1,3,4-thiadiazol-2-ylbenzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 4 h / 90 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 65 °C

3: dichloromethane / 1 h / 20 °C

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;