Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

Base Information

Chemical Name:Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester
CAS No.:164988-71-0
Molecular Formula:C₃₇H₅₂O₆S
Molecular Weight:624.882
Hs Code.:

Synonyms:Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

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Chemical Property of Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

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Technology Process of Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

There total 6 articles about Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-29-8
1-bromo dodecane

: 164988-71-0
Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 12 h / 150 °C

2: 1.) nBuLi / 1.) hexane, THF, -10 deg C, 30 min, 2.) hexane, THF, RT, 16 h

3: H₂ / 10percent Pd/C / tetrahydrofuran / 16 h

4: pyridine / 1.5 h / 20 °C

With pyridine; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00012a018

Reference yield:

: 20672-66-6,40246-26-2,84926-76-1,114179-79-2,115184-49-1
3,4,5-tri-O-benzyl-D-galactopyranose

: 164988-71-0
Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄ / ethanol; H₂O / 16 h / -5 - 20 °C

2: 1.) nBuLi / 1.) hexane, THF, -10 deg C, 30 min, 2.) hexane, THF, RT, 16 h

3: H₂ / 10percent Pd/C / tetrahydrofuran / 16 h

4: pyridine / 1.5 h / 20 °C

With pyridine; sodium periodate; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00012a018

Reference yield:

: 115563-43-4
(2S,3S,4R)-2,3,5-tribenzyloxy-4-hydroxypentanal

: 164988-71-0
Methanesulfonic acid (1R,2R,3R)-2,3-bis-benzyloxy-1-benzyloxymethyl-tetradecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) nBuLi / 1.) hexane, THF, -10 deg C, 30 min, 2.) hexane, THF, RT, 16 h

2: H₂ / 10percent Pd/C / tetrahydrofuran / 16 h

3: pyridine / 1.5 h / 20 °C

With pyridine; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00012a018