Technology Process of C24H31N5O4
There total 3 articles about C24H31N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.17 h / 20 °C
1.2: 24 h / 20 °C
2.1: palladium on activated charcoal; hydrogen / methanol / 4 h / 20 °C / 1500.15 Torr
3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.17 h / 20 °C
3.2: 48 h / 20 °C
4.1: sodium acetate / methanol / 48 h / 20 °C
With
dmap; palladium on activated charcoal; hydrogen; sodium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2012.09.086
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: piperdinium acetate / ethanol / 2.33 h / 20 °C / Reflux
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.17 h / 20 °C
2.2: 48 h / 20 °C
3.1: sodium acetate / methanol / 48 h / 20 °C
With
dmap; sodium acetate; piperdinium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.bmcl.2012.09.086