(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

Base Information

Chemical Name:(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate
CAS No.:1292309-91-1
Molecular Formula:C₃₈H₅₂N₂O₁₁S
Molecular Weight:744.904
Hs Code.:

Synonyms:(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

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Chemical Property of (E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

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Technology Process of (E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

There total 8 articles about (E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1292309-90-0
(E)-tert-butyl 4-(2-(6-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethoxy)pyridin-3-yl)vinyl)phenyl(methyl)carbamate

: 7460-82-4
diethylene glycol ditosylate

: 1292309-91-1
(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm2009106

Reference yield:

: 69045-79-0
2-choro-5-iodopyridine

: 1292309-91-1
(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 150 °C / Microwave irradiation

2: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide

With tetrabutylammomium bromide; palladium diacetate; sodium hydride; potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm2009106

Reference yield:

: 937183-61-4
4-N-(tert-butyloxycarbonyl)-4-N-methylaminostyrene

: 1292309-91-1
(E)-17-(5-(4-(tert-butoxycarbonyl(methyl)amino)styryl)pyridin-2-yloxy)-3,6,9,12,15-pentaoxaheptadecyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide

With tetrabutylammomium bromide; palladium diacetate; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm2009106