3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Base Information

Chemical Name:3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)
CAS No.:331241-61-3
Molecular Formula:C₃₇H₆₆FO₁₄P₃
Molecular Weight:846.842
Hs Code.:

Synonyms:3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Suppliers and Price of 3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

There total 8 articles about 3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzoic acid (1R,2R,3R,5S,6S)-2,3,5-tris-(dibutoxy-phosphanyloxy)-6-fluoro-cyclohexyl ester

: 331241-61-3
3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Guidance literature:: With tert.-butylhydroperoxide; In dichloromethane; acetonitrile; at 20 ℃; for 20h;
DOI:10.1016/S0040-4020(00)01112-1

Reference yield:

: 156593-40-7
D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol

: 331241-61-3
3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / sodium hydride / dimethylformamide / 12 h

2: 98 percent / aq. HCl / methanol / 15 h / 60 °C

3: 80 percent / pyridine / 0.33 h / 10 °C

4: 90 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 2 h / 20 °C

5: 100 percent / hydrogen / Pd/C / ethyl acetate; ethanol / 2 h / 155.14 Torr

6: 1H-tetrazole / acetonitrile / 3 h

7: t-BuOOH / acetonitrile; CH₂Cl₂ / 20 h / 20 °C

With pyridine; 1H-tetrazole; hydrogenchloride; tert.-butylhydroperoxide; diethylamino-sulfur trifluoride; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(00)01112-1

Reference yield:

: 331241-52-2
1,4,5-tri-O-benzyl-6-deoxy-D-myo-inositol

: 331241-61-3
3-O-benzoyl-2,6-dideoxy-2-fluoro-scyllo-inositol 1,4,5-tris(dibutyl phosphate)

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / pyridine / 0.33 h / 10 °C

2: 90 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 2 h / 20 °C

3: 100 percent / hydrogen / Pd/C / ethyl acetate; ethanol / 2 h / 155.14 Torr

4: 1H-tetrazole / acetonitrile / 3 h

5: t-BuOOH / acetonitrile; CH₂Cl₂ / 20 h / 20 °C

With pyridine; 1H-tetrazole; tert.-butylhydroperoxide; diethylamino-sulfur trifluoride; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4020(00)01112-1