Dibutyl diisopropylamidophosphite

Base Information

Chemical Name:Dibutyl diisopropylamidophosphite
CAS No.:63815-59-8
Molecular Formula:C₁₄H₃₂NO₂P
Molecular Weight:277.387
Hs Code.:
DSSTox Substance ID:DTXSID40980397
Wikidata:Q82966334

Synonyms:63815-59-8;Dibutyl diisopropylamidophosphite;Phosphoramidous acid, N,N-diisopropyl-, dibutyl ester;SCHEMBL3634742;DTXSID40980397;Dibutyl N,N-dipropan-2-ylphosphoramidoite

Suppliers and Price of Dibutyl diisopropylamidophosphite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Dibutyl diisopropylamidophosphite

Chemical Property:

Vapor Pressure:0.00848mmHg at 25°C
Boiling Point:266.8°C at 760 mmHg
Flash Point:115.1°C
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:11
Exact Mass:277.21706626
Heavy Atom Count:18
Complexity:171

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOP(N(C(C)C)C(C)C)OCCCC

Technology Process of Dibutyl diisopropylamidophosphite

There total 2 articles about Dibutyl diisopropylamidophosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 921-26-6
N,N-diisopropylphosphoramide dichloride

: 71-36-3
butan-1-ol

: 63815-59-8
O,O-dibutyl-N,N-diisopropylphosphoramidite

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In hexane; at -50 - 20 ℃;
DOI:10.1002/ejoc.200700521

Reference yield:

: 108-18-9
diisopropylamine

: 63815-59-8
O,O-dibutyl-N,N-diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: 6.3 g / PCl₃ / diethyl ether / -10 - 20 °C

2: ethyl diisopropylamine / acetonitrile / -10 - 20 °C

With N-ethyl-N,N-diisopropylamine; phosphorus trichloride; In diethyl ether; acetonitrile; 1: Addition / 2: Substitution;
DOI:10.1016/S0040-4020(99)00365-8

Reference yield: 55.0%

: 63815-59-8
O,O-dibutyl-N,N-diisopropylphosphoramidite

: 160765-31-1
D-2-O-benzyl-6-deoxy-myo-inositol

: D-2-O-benzyl-6-deoxy-myo-inositol-1,3,4,5-tetrakis(dibutyl)phosphate

Guidance literature:: O,O-dibutyl-N,N-diisopropylphosphoramidite; D-2-O-benzyl-6-deoxy-myo-inositol; With 1H-tetrazole;

With tert.-butylhydroperoxide;
DOI:10.1016/S0040-4020(99)00366-X