methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

Base Information

• Chemical Name: methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside
• CAS No.: 85687-32-7
• Molecular Formula: C₁₇H₂₀F₃NO₅
• Molecular Weight: 375.345

Synonyms:methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

Chemical Property of methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

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Technology Process of methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

There total 13 articles about methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside (85687-30-5) → methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside (85687-32-7)

Guidance literature:

With hydrogen; triethylamine; nickel; In isopropyl alcohol; for 15h; Ambient temperature;

DOI:10.1021/jo00066a029

Reference yield: 90.0%

methyl 4-O-benzoyl-2,3,6-trideoxy-6-iodo-3-C-methyl-3-trifluoroacetamido-α-D-ribo-hexopyranoside (85687-31-6) → methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside (85687-32-7)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; for 4h; Ambient temperature;

Reference yield: 4.0%

methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-α-D-erythro-hex-5-enopyranoside (95086-98-9) → methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside (95086-99-0) + methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside (85687-32-7)

Guidance literature:

With hydrogen; nickel; In ethanol;

DOI:10.1016/S0008-6215(00)90775-4

upstream raw materials:

methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-α-D-erythro-hex-5-enopyranoside

methyl 4-O-benzoyl-2,3,6-trideoxy-6-iodo-3-C-methyl-3-trifluoroacetamido-α-D-ribo-hexopyranoside

methyl 4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

methyl 4,6-O-(R)-benzylidene-2-deoxy-α-D-erythrohexopyranosid-3-ulose

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