methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

Base Information

Chemical Name:methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside
CAS No.:95086-99-0
Molecular Formula:C₁₇H₂₀F₃NO₅
Molecular Weight:375.345
Hs Code.:

Synonyms:methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

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Technology Process of methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

There total 8 articles about methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 95086-98-9
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-α-D-erythro-hex-5-enopyranoside

: 95086-99-0
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 12h;
DOI:10.1055/s-2006-926231

Reference yield: 4.0%

: 95086-98-9
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-α-D-erythro-hex-5-enopyranoside

: 95086-99-0
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

: 85687-32-7
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

Guidance literature:: With hydrogen; nickel; In ethanol;
DOI:10.1016/S0008-6215(00)90775-4

Reference yield:

: 85687-30-5
methyl 4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-3-(trifluoroacetamido)-α-D-ribo-hexopyranoside

: 95086-99-0
methyl 4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-3-trifluoroacetamido-β-L-lyxohexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / DBU / dimethylformamide / 4 h / 90 °C

2: 67 percent / H₂ / Pd/C / methanol / 12 h / 20 °C

With hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-926231