C₂₃H₂₈FN₅O₅Si

Base Information

Chemical Name:C₂₃H₂₈FN₅O₅Si
CAS No.:1412911-81-9
Molecular Formula:C₂₃H₂₈FN₅O₅Si
Molecular Weight:501.59
Hs Code.:

C<sub>23</sub>H<sub>28</sub>FN<sub>5</sub>O<sub>5</sub>Si

Synonyms:C₂₃H₂₈FN₅O₅Si

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Chemical Property of C₂₃H₂₈FN₅O₅Si

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Technology Process of C₂₃H₂₈FN₅O₅Si

There total 6 articles about C₂₃H₂₈FN₅O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1048373-98-3
C₂₃H₃₀FN₅O₄Si

: 1412911-85-3
C₁₇H₁₄FN₅O₅

: 1412911-81-9
C₂₃H₂₈FN₅O₅Si

Guidance literature:: C₂₃H₃₀FN₅O₄Si; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; acetic acid; In water; acetonitrile; at 22 - 40 ℃; for 0.25h;

With [bis(acetoxy)iodo]benzene; acetic acid; In water; acetonitrile; at 22 ℃; for 0.25h; pH=6.5 - 7;

Reference yield:

: 144924-99-2
N-(9-((2R,3S,4R,5R)-3-fluoro-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)-9H-purin-6-yl)benzamide

: 1412911-81-9
C₂₃H₂₈FN₅O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / toluene / 50 °C

2.1: toluene-4-sulfonic acid / toluene; methanol / 0 °C

3.1: sodium hydrogencarbonate; acetic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 0.25 h / 22 - 40 °C

3.2: 0.25 h / 22 °C / pH 6.5 - 7

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; water; toluene; acetonitrile;

Reference yield:

: 4005-49-6
N-benzoyladenine

: 1412911-81-9
C₂₃H₂₈FN₅O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; acetic acid / dichloromethane / 0 °C

1.2: Reflux

1.3: 0.5 h / 22 °C

2.1: sodium hydroxide / water; tetrahydrofuran / 3 °C

2.2: 1 h / 3 - 22 °C / pH 6 - 7

3.1: N-ethyl-N,N-diisopropylamine / toluene / 50 °C

4.1: toluene-4-sulfonic acid / toluene; methanol / 0 °C

5.1: sodium hydrogencarbonate; acetic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 0.25 h / 22 - 40 °C

5.2: 0.25 h / 22 °C / pH 6.5 - 7

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrogen bromide; sodium hydrogencarbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile;