11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Base Information

Chemical Name:11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid
CAS No.:119802-49-2
Molecular Formula:C₄₀H₅₀Cl₂O₄S₆
Molecular Weight:858.137
Hs Code.:

Synonyms:11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Suppliers and Price of 11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

There total 4 articles about 11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 127679-23-6
11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

: 119802-49-2
11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Guidance literature:: With trichloroacetic acid; In benzene; for 1h; Heating;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 119802-49-2
11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / Heating

2: 1.) NaBH₄, 2.) 12N HCl / 1.) 10 min, with ice cooling, 2.) 1h, room temperature

3: 66 percent / trichloroacetic acid / benzene / 1 h / Heating

With hydrogenchloride; sodium tetrahydroborate; trichloroacetic acid; In acetone; benzene;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 84969-93-7,85102-63-2
C₁₄H₁₄ClNS₃

: 119802-49-2
11-[(E)-4'-(10-Carboxy-decylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-undecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / Heating

2: 1.) NaBH₄, 2.) 12N HCl / 1.) 10 min, with ice cooling, 2.) 1h, room temperature

3: 66 percent / trichloroacetic acid / benzene / 1 h / Heating

With hydrogenchloride; sodium tetrahydroborate; trichloroacetic acid; In acetone; benzene;
DOI:10.1016/S0040-4020(01)85427-2