11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

Base Information

Chemical Name:11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid
CAS No.:127679-23-6
Molecular Formula:C₂₂H₃₁ClO₃S₃
Molecular Weight:475.137
Hs Code.:

Synonyms:11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

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Chemical Property of 11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

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Technology Process of 11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

There total 3 articles about 11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 127679-23-6
11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / Heating

2: 1.) NaBH₄, 2.) 12N HCl / 1.) 10 min, with ice cooling, 2.) 1h, room temperature

With hydrogenchloride; sodium tetrahydroborate; In acetone;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 84969-93-7,85102-63-2
C₁₄H₁₄ClNS₃

: 127679-23-6
11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / Heating

2: 1.) NaBH₄, 2.) 12N HCl / 1.) 10 min, with ice cooling, 2.) 1h, room temperature

With hydrogenchloride; sodium tetrahydroborate; In acetone;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 64-17-5
ethanol

: 11-[5-(4-Chloro-phenyl)-2-piperidin-1-yl-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

: 127679-23-6
11-[5-(4-Chloro-phenyl)-2-ethoxy-[1,3]dithiol-4-ylsulfanyl]-undecanoic acid

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; 1.) 10 min, with ice cooling, 2.) 1h, room temperature;
DOI:10.1016/S0040-4020(01)85427-2