6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

Base Information

Chemical Name:6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone
CAS No.:160008-40-2
Molecular Formula:C₂₇H₂₆BrN₃O₉
Molecular Weight:616.422
Hs Code.:

6-bromo-2-phenyl-3-<N-acetyl-N-(tri-O-acetyl-β-D-xylopyranosyl)>amino-4(3H)-quinazolinone

Synonyms:6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

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Chemical Property of 6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

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Technology Process of 6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

There total 6 articles about 6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 108-24-7
acetic anhydride

: 160008-39-9
6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

: 160008-40-2
6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

Guidance literature:: With pyridine; for 24h; Ambient temperature;

Reference yield:

: 115754-65-9
6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

: 160008-40-2
6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / AcOH / methanol / 2.25 h / Heating

2: 66 percent / pyridine / 24 h / Ambient temperature

With pyridine; acetic acid; In methanol;

Reference yield:

: 3068-31-3
1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose

: 160008-40-2
6-bromo-2-phenyl-3-amino-4(3H)-quinazolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 23.7 percent / acetone / 48 h / Ambient temperature

2: pyridine

With pyridine; In acetone;