N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine
CAS No.:801300-47-0
Molecular Formula:C₂₄H₃₂N₄O₂
Molecular Weight:408.544
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

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Chemical Property of N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

Chemical Property:

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Technology Process of N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

There total 3 articles about N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 801300-46-9
N-(tert-butoxycarbonyl)-N-(4-chloromethylbenzyl)-4-tert-butylbenzylamine

: 801300-47-0
N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

Guidance literature:: With sodium azide; In butanone; for 120h; Heating;
DOI:10.1021/ol0484557

Reference yield:

: 477884-47-2
4-{[tert-butoxycarbonyl-(4-tert-butyl-benzyl)-amino]-methyl}-benzoic acid methyl ester

: 801300-47-0
N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2: 78 percent / Ph₃P; N-chlorosuccinimide / tetrahydrofuran

3: NaN₃ / butan-2-one / 120 h / Heating

With N-chloro-succinimide; lithium aluminium tetrahydride; sodium azide; triphenylphosphine; In tetrahydrofuran; butanone;
DOI:10.1021/ol0484557

Reference yield:

: 801300-45-8
N-(tert-butoxycarbonyl)-N-(4-hydroxymethylbenzyl)-4-tert-butylbenzylamine

: 801300-47-0
N-(tert-butoxycarbonyl)-N-(4-azidomethylbenzyl)-4-tert-butylbenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / Ph₃P; N-chlorosuccinimide / tetrahydrofuran

2: NaN₃ / butan-2-one / 120 h / Heating

With N-chloro-succinimide; sodium azide; triphenylphosphine; In tetrahydrofuran; butanone;
DOI:10.1021/ol0484557