PENTANEDIOIC-3,3-D2 ACID

Base Information

• Chemical Name: PENTANEDIOIC-3,3-D2 ACID
• CAS No.: 43087-19-0
• Molecular Formula: C₅H₈O₄
• Molecular Weight: 134.1
• Mol file: 43087-19-0.mol

Synonyms:PENTANEDIOIC-3,3-D2 ACID

Chemical Property of PENTANEDIOIC-3,3-D2 ACID

Chemical Property:

• PSA: 74.60000
• LogP: 0.32590

Purity/Quality:

99% ^*data from raw suppliers

Pentanedioic-3,3-d2Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Pentanedioic-3,3-d2 Acid (CAS# 43087-19-0) is a useful isotopically labeled research compound.

Technology Process of PENTANEDIOIC-3,3-D2 ACID

There total 3 articles about PENTANEDIOIC-3,3-D2 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-glutamic acid (56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6) → <3,3-2H2>glutaric acid (43087-19-0)

Guidance literature:

With water-d2; potassium hydroxide; at 37 ℃; for 4h; pH=13;

DOI:10.1002/anie.202105667

Reference yield:

1,3-dibromo<2,2-2H2>propane (38645-15-7) + potassium cyanide (151-50-8) → <3,3-2H2>glutaric acid (43087-19-0)

Guidance literature:

With sulfuric acid; Yield given. Multistep reaction; 1.) ethanol, reflux, 35 h;

Reference yield:

→ <3,3-2H2>glutaric acid (43087-19-0)

Guidance literature:

2,2-Dideuteropropan-1,1,3,3-tetra-(carbonsaeureaethylester), Hydrolyse, Decarboxy-lierung;

DOI:10.1002/jlcr.2590090217

upstream raw materials:

1,3-dibromo<2,2-2H2>propane

potassium cyanide

L-glutamic acid

Refernces

• 1、 Cocker, Wesley,Geraghty, Niall W. A.,McMurry, T. Brian H.,Shannon, Patrick V. R.. "An Investigation of the Thermal Decomposition of the Methohydroxides and Methodeuterio-oxides of Some 5-N,N-Dimethylaminopent-1-enes". . p. 2245 - 2254. Retrieved 2007/10/02.