6-MeO-BTA-0

Base Information

• Chemical Name: 6-MeO-BTA-0
• CAS No.: 43036-17-5
• Molecular Formula: C14H12 N2 O S
• Molecular Weight: 256.328
• Hs Code.: 2934999090
• Mol file: 43036-17-5.mol

Synonyms:2-(4-Aminophenyl)-6-methoxybenzothiazole;4-(6-Methoxybenzothiazol-2-yl)aniline; 4-(6-Methoxybenzothiazol-2-yl)phenylamine;6-Methoxy-2-(4-aminophenyl)benzothiazole

Chemical Property of 6-MeO-BTA-0

Chemical Property:

• PSA: 76.38000
• LogP: 4.13530

Purity/Quality:

99.90% ^*data from raw suppliers

4-(6-Methoxybenzothiazol-2-yl)-phenylamine 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-MeO-BTA-0

There total 22 articles about 6-MeO-BTA-0 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

6-methoxy-2-(4-nitrophenyl)benzothiazole (43036-14-2) → 2-(4-aminophenyl)-6-methoxybenzothiazole (43036-17-5)

Guidance literature:

With tin(ll) chloride; In ethanol; for 4h; Reflux; Inert atmosphere;

Reference yield: 88.0%

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) + 2-amino-5-methoxy-thiophenol (6274-29-9) → 2-(4-aminophenyl)-6-methoxybenzothiazole (43036-17-5)

Guidance literature:

With melamine formaldehyde resin supported sulfuric acid; Microwave irradiation;

DOI:10.1134/S1070363215030251

Reference yield: 68.0%

6-methoxy-1,3-benzothiazole (2942-13-4) + tert-butyl (4-bromophenyl)carbamate (131818-17-2) → 2-(4-aminophenyl)-6-methoxybenzothiazole (43036-17-5) + [4-(6-methoxy-benzothiazol-2-yl)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:

With caesium carbonate; copper(I) bromide; Pd(OAc)2*P(t-Bu)3; In N,N-dimethyl-formamide; at 150 ℃; for 1h;

DOI:10.1016/j.tetlet.2004.12.111

upstream raw materials:

6-methoxy-2-(4-nitrophenyl)benzothiazole

6-methoxy-1,3-benzothiazole

4-bromo-aniline

tert-butyl (4-bromophenyl)carbamate

Downstream raw materials:

2-(4’-aminophenyl)-6-hydroxybenzothiazole

2-(4-amino-3-iodophenyl)-6-methoxybenzothiazole

4-(6-methoxybenzo[d]thiazol2-yl)-N,N-dimethylaniline

2-(4-amino-3-chlorophenyl)-6-methoxybenzothiazole