4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Base Information

Chemical Name:4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane
CAS No.:1276543-48-6
Molecular Formula:C₃₂H₅₃N₅O₆
Molecular Weight:603.803
Hs Code.:

Synonyms:4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Suppliers and Price of 4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

There total 10 articles about 4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 134439-25-1
2-[(4-nitrophenyl)methyl]propan-1,3-diol bis(4-methylbenzenesulfonate)

: 852921-64-3
1,8-N,N′-bis(carbo-tert-butoxymethyl)-1,4,8,11-tetraazacyclotetradecane

: 1276543-48-6
4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Guidance literature:: With sodium carbonate; In toluene; for 144h; Reflux;

Reference yield:

: 7598-70-1
diethyl 2-(4-nitrobenzyl)malonate

: 1276543-48-6
4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 16 h / Reflux

2: pyridine / 10 h / 0 - 20 °C

3: sodium carbonate / toluene / 144 h / Reflux

With pyridine; sodium tetrahydroborate; sodium carbonate; In ethanol; toluene;

Reference yield:

: 73344-98-6
2-[(4-nitrophenyl)methyl]propan-1,3-diol

: 1276543-48-6
4,11-N,N'-bis(carbo-tert-butoxymethyl)-16-(4-nitrobenzyl)-1,4,8,11-tetraazabicyclo[6.6.3]heptadecane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 10 h / 0 - 20 °C

2: sodium carbonate / toluene / 144 h / Reflux

With pyridine; sodium carbonate; In toluene;