3,3’-(5-chloro-1,3-phenylene)dipyridine

Base Information Edit

Chemical Name:3,3’-(5-chloro-1,3-phenylene)dipyridine
CAS No.:1214345-76-2
Molecular Formula:C₁₆H₁₁ClN₂
Molecular Weight:266.73
Hs Code.:
Mol file:1214345-76-2.mol

Synonyms:3,3’-(5-chloro-1,3-phenylene)dipyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3’-(5-chloro-1,3-phenylene)dipyridine Edit

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Technology Process of 3,3’-(5-chloro-1,3-phenylene)dipyridine

There total 2 articles about 3,3’-(5-chloro-1,3-phenylene)dipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 1692-25-7
3-pyridylboronic acid

: 1214345-76-2
3,3’-(5-chloro-1,3-phenylene)dipyridine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 100 ℃; Inert atmosphere;

Reference yield:

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 329214-79-1
3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 1214345-76-2
3,3’-(5-chloro-1,3-phenylene)dipyridine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; for 8h;
DOI:10.1016/j.orgel.2019.105498