tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

Base Information

Chemical Name:tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate
CAS No.:1373613-92-3
Molecular Formula:C₁₉H₂₇NO₆
Molecular Weight:365.426
Hs Code.:

Synonyms:tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

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Chemical Property of tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

Chemical Property:

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Technology Process of tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

There total 3 articles about tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163116-18-5
N-ethoxycarbonylmethyl-β-alanine t-butyl ester

: 501-53-1,94274-21-2
benzyl chloroformate

: 1373613-92-3
tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; at 20 - 33 ℃; for 2h;

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 623-33-6
glycine ethyl ester hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 1373613-92-3
tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

Guidance literature:: tert-Butyl acrylate; glycine ethyl ester hydrochloride; With triethylamine; In water; isopropyl alcohol; at 30 - 64 ℃;

benzyl chloroformate; With sodium hydrogencarbonate; In water; ethyl acetate; at 25 - 36 ℃; for 2h;

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1373613-92-3
tert-butyl 3-{N-benzyloxycarbonyl-N-(ethoxycarbonylmethyl)amino}propionate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / water; isopropyl alcohol / 7 h / 59 - 63 °C

2: sodium hydrogencarbonate / water; ethyl acetate / 2 h / 20 - 33 °C

With sodium hydrogencarbonate; triethylamine; In water; ethyl acetate; isopropyl alcohol;