C₄₀H₄₆N₄O₄S

Base Information

Chemical Name:C₄₀H₄₆N₄O₄S
CAS No.:1255150-34-5
Molecular Formula:C₄₀H₄₆N₄O₄S
Molecular Weight:678.896
Hs Code.:

C<sub>40</sub>H<sub>46</sub>N<sub>4</sub>O<sub>4</sub>S

Synonyms:C₄₀H₄₆N₄O₄S

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Chemical Property of C₄₀H₄₆N₄O₄S

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Technology Process of C₄₀H₄₆N₄O₄S

There total 9 articles about C₄₀H₄₆N₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1255150-33-4
C₅₂H₇₆N₄O₄SSi₂

: 1255150-34-5
C₄₀H₄₆N₄O₄S

Guidance literature:: C₅₂H₇₆N₄O₄SSi₂; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

With silver(l) oxide; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 16292-17-4
bis(4-bromophenyl)amine

: 1255150-34-5
C₄₀H₄₆N₄O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: tert.-butyl lithium / diethyl ether / 3 h / -78 - 20 °C

1.2: 3 h / -78 - 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 10 h / 20 °C

3.1: piperidine; sodium t-butanolate / copper(l) iodide / toluene / 5 h / Reflux; Inert atmosphere

4.1: sodium t-butanolate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / Reflux; Inert atmosphere

5.1: piperidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 5 h / Reflux; Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

6.2: 2 h / 20 °C / Inert atmosphere

With piperidine; 1H-imidazole; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium t-butanolate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1693-86-3
3-hexylthiophene

: 1255150-34-5
C₄₀H₄₆N₄O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide / tetrachloromethane / 3 h / 20 °C

2.1: tert.-butyl lithium / Dimethyl ether / 3 h / -78 - 20 °C

2.2: 12 h / -78 - 20 °C

3.1: sodium t-butanolate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / Reflux; Inert atmosphere

4.1: piperidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 5 h / Reflux; Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

With piperidine; N-Bromosuccinimide; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; Dimethyl ether; toluene;