C₂₃H₃₀O₂

Base Information

Chemical Name:C₂₃H₃₀O₂
CAS No.:756834-58-9
Molecular Formula:C₂₃H₃₀O₂
Molecular Weight:338.49
Hs Code.:

C<sub>23</sub>H<sub>30</sub>O<sub>2</sub>

Synonyms:C₂₃H₃₀O₂

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Chemical Property of C₂₃H₃₀O₂

Chemical Property:

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Technology Process of C₂₃H₃₀O₂

There total 6 articles about C₂₃H₃₀O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-39-0
benzyl bromide

: 756834-65-8
(4R,7S)-8-Benzyloxy-7-methyl-oct-1-en-4-ol

: 756834-58-9
C₂₃H₃₀O₂

Guidance literature:: (4R,7S)-8-Benzyloxy-7-methyl-oct-1-en-4-ol; With potassium hydride; In tetrahydrofuran; at 0 ℃; for 0.333333h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 0 - 20 ℃; for 48h;
DOI:10.1021/ja101811x

Reference yield:

: 63930-46-1
(S)-3-benzyloxy-2-methylpropan-1-ol

: 756834-58-9
C₂₃H₃₀O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 93 percent / pyridine / CH₂Cl₂ / 20.3 h / 20 °C

2.1: 82 percent / CuCl / diethyl ether / 12 h / 20 °C

3.1: aq. NMO; OsO₄ / 2-methyl-propan-2-ol; tetrahydrofuran / 16 h / 20 °C

4.1: 4.9 g / Pb(OAc)4 / ethyl acetate / 0 °C

5.1: 4.4 g / aq. NaOH; H₂O₂ / diethyl ether / 12 h

6.1: KH / tetrahydrofuran / 0.33 h / 0 °C

6.2: 79 percent / Bu₄NI / tetrahydrofuran / 18 h / 20 °C

With pyridine; lead(IV) acetate; sodium hydroxide; osmium(VIII) oxide; N-methyl-2-indolinone; dihydrogen peroxide; potassium hydride; copper(l) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/ja046588h

Reference yield:

: 90367-65-0
(2R)-1-(Benzyloxy)-2-methyl-3-(p-toluenesulfonyloxy)propane

: 756834-58-9
C₂₃H₃₀O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 82 percent / CuCl / diethyl ether / 12 h / 20 °C

2.1: aq. NMO; OsO₄ / 2-methyl-propan-2-ol; tetrahydrofuran / 16 h / 20 °C

3.1: 4.9 g / Pb(OAc)4 / ethyl acetate / 0 °C

4.1: 4.4 g / aq. NaOH; H₂O₂ / diethyl ether / 12 h

5.1: KH / tetrahydrofuran / 0.33 h / 0 °C

5.2: 79 percent / Bu₄NI / tetrahydrofuran / 18 h / 20 °C

With lead(IV) acetate; sodium hydroxide; osmium(VIII) oxide; N-methyl-2-indolinone; dihydrogen peroxide; potassium hydride; copper(l) chloride; In tetrahydrofuran; diethyl ether; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/ja046588h