Technology Process of C24H31NO6
There total 9 articles about C24H31NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium fluoride;
In
isopropyl alcohol;
at 20 ℃;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaIO4; NaHCO3 / methanol; H2O / 1 h / 0 °C
2: 1.28 g / KF / propan-2-ol / 20 °C
With
potassium fluoride; sodium periodate; sodium hydrogencarbonate;
In
methanol; water; isopropyl alcohol;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 45 percent / (-)-diisopropyl tartrate; Ti(Oi-Pr)4; tert-butyl hydroperoxide / CH2Cl2; decane
2: 50 percent / BF3*Et2O / CH2Cl2 / 15 h / 20 °C
3: 81 percent / potassium carbonate / methanol / 1 h / 20 °C
4: 95 percent / aq. HClO4 / dimethylsulfoxide / 5 h / 80 °C
5: NaIO4; NaHCO3 / methanol; H2O / 1 h / 0 °C
6: 1.28 g / KF / propan-2-ol / 20 °C
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; potassium fluoride; sodium periodate; perchloric acid; (-)-diisopropyl tartrate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate;
In
methanol; decane; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1021/ol0701013