zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

Base Information

Chemical Name:zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin
CAS No.:179690-80-3
Molecular Formula:C₄₂H₄₃BrN₄O₄Zn
Molecular Weight:813.122
Hs Code.:

Synonyms:zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

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Chemical Property of zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

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Technology Process of zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

There total 1 articles about zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.8%

: 557-34-6
zinc diacetate

: 131353-85-0
5-(4-Bromophenyl)-2,8-diethyl-3,7-dimethyldihydrodipyrrin

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 179690-80-3
zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

Guidance literature:: With air; toluene-4-sulfonic acid; In dichloromethane; di-unsubstituted dipyrrine soln. (CH2Cl2) stirring 15 min, mixing with other org. compds. soln. (MeOH), stirring overnight (N2), Zn-salt soln. (MeOH) addn., stirring 12 h (slow air stream bubbling through soln.), washing (water, aq. NaHCO3), evapn.; residue column chromy. (alumina, CH2Cl2);

Reference yield: 64.0%

: 179690-80-3
zinc(II) 5-(4-bromophenyl)-2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethylporphyrin

: 7486-35-3
tri-n-butyl(vinyl)tin

: 179690-82-5
zinc(II) 2,8-diethyl-13,17-bis(methoxycarbonylethyl)-3,7,12,18-tetramethyl-5-(4-vinylphenyl)porphyrin

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; mixt. refluxing 10 h, cooling to room temp.; residue column chromy. (alumina, 0.5% CH3OH/CH2Cl2);