endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

Base Information

Chemical Name:endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en
CAS No.:73642-70-3
Molecular Formula:C₁₈H₂₂O₃
Molecular Weight:286.371
Hs Code.:

Synonyms:endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

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Chemical Property of endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

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Technology Process of endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

There total 3 articles about endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 107-21-1
ethylene glycol

: 73642-48-5
exo-2-Benzyloxybicyclo<2.2.1>hept-5-en-3-yl-endo-1-ethanon

: 73642-70-3
endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 24h; Heating;

Reference yield:

: 73642-47-4
(E)-4-Benzyloxybut-3-en-2-one

: 73642-70-3
endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SnCl₄ / CH₂Cl₂ / 15 h / Ambient temperature

2: 89 percent / p-TsOH / toluene / 24 h / Heating

With tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane; toluene;

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 73642-70-3
endo-3-(2-Methyl-1,3-dioxolan-2-yl)-exo-2-benzyloxybicyclo<2.2.1>hept-5-en

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SnCl₄ / CH₂Cl₂ / 15 h / Ambient temperature

2: 89 percent / p-TsOH / toluene / 24 h / Heating

With tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane; toluene;