(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

Base Information

Chemical Name:(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine
CAS No.:1612876-13-7
Molecular Formula:C₂₇H₁₈FNOSe
Molecular Weight:470.404
Hs Code.:

Synonyms:(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

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Technology Process of (Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

There total 3 articles about (Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 52673-29-7
4,4'-difluorodiphenyl diselenide

: 104682-98-6
N-(2-(2-phenylethynyl)phenyl)benzamide

: 1612876-13-7
(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

Guidance literature:: 4,4'-difluorodiphenyl diselenide; With iron(III) chloride; In dichloromethane; at 20 ℃; Schlenk technique; Inert atmosphere;

N-(2-(2-phenylethynyl)phenyl)benzamide; In dichloromethane; at 20 ℃; for 1h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201300925

Reference yield:

: 13141-38-3
2-phenylethynylaniline

: 1612876-13-7
(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

2.1: iron(III) chloride / dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

2.2: 1 h / 20 °C / Schlenk technique; Inert atmosphere

With iron(III) chloride; In dichloromethane;
DOI:10.1002/adsc.201300925

Reference yield:

: 98-88-4
benzoyl chloride

: 1612876-13-7
(Z)-4-((p-fluorophenylseleno)(phenyl)methylene)-2-phenyl-4H-benzo[d][1,3]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

2.1: iron(III) chloride / dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

2.2: 1 h / 20 °C / Schlenk technique; Inert atmosphere

With iron(III) chloride; In dichloromethane;
DOI:10.1002/adsc.201300925