(S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate

Base Information

• Chemical Name: (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate
• CAS No.: 951328-86-2
• Molecular Formula: C₁₈H₂₅N₃O₃S
• Molecular Weight: 363.481

Synonyms:(S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate

Chemical Property of (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate

Chemical Property:

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Technology Process of (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate

There total 1 articles about (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butyloxycarbonyl)-S-methylisothiourea (173998-77-1) + (S)-1-phenylpyrrolidine-2-carboxylic acid (139983-29-2) → (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate (951328-86-2)

Guidance literature:

With 4-methyl-morpholine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 87.0%

4-(aminomethyl)-2,6-dichloroaniline (164648-75-3) + (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate (951328-86-2) → (S)-tert-butyl N-(4-amino-3,5-dichlorobenzyl)-N'-(1-phenylpyrrolidine-5-carbonyl)carbamimidoylcarbamate (951329-10-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield: 76.0%

3,5-dichloro-4-acetamidobenzylamine (918451-59-9) + (S)-tert-butyl methylthio-N-(1-phenylpyrrolidine-5-carbonyl)carbonoimidoylcarbamate (951328-86-2) → (S)-tert-butyl N-(4-acetamido-3,5-dichlorobenzyl)-N'-(1-phenylpyrrolidine-5-carbonyl)carbamimidoylcarbamate (951329-12-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

upstream raw materials:

N-(tert-butyloxycarbonyl)-S-methylisothiourea

(S)-1-phenylpyrrolidine-2-carboxylic acid

Downstream raw materials:

(S)-tert-butyl N-(4-amino-3,5-dichlorobenzyl)-N'-(1-phenylpyrrolidine-5-carbonyl)carbamimidoylcarbamate

(S)-tert-butyl N-(4-acetamido-3,5-dichlorobenzyl)-N'-(1-phenylpyrrolidine-5-carbonyl)carbamimidoylcarbamate

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