Technology Process of C17H23FN4
There total 5 articles about C17H23FN4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / 3 h / Reflux
2.1: sodium hydride / dimethyl sulfoxide / 20 - 85 °C / Inert atmosphere
2.2: 12 h / 20 - 85 °C / Inert atmosphere
3.1: sodium hydroxide / diethyl ether / Cooling with ice
4.1: potassium iodide; sodium carbonate / acetonitrile; N,N-dimethyl-formamide / 2 h / 60 °C
5.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 20 °C
With
pyridine; lithium aluminium tetrahydride; sodium hydride; sodium carbonate; potassium iodide; sodium hydroxide;
In
diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3390/molecules181114186
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / dimethyl sulfoxide / 20 - 85 °C / Inert atmosphere
1.2: 12 h / 20 - 85 °C / Inert atmosphere
2.1: sodium hydroxide / diethyl ether / Cooling with ice
3.1: potassium iodide; sodium carbonate / acetonitrile; N,N-dimethyl-formamide / 2 h / 60 °C
4.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 20 °C
With
lithium aluminium tetrahydride; sodium hydride; sodium carbonate; potassium iodide; sodium hydroxide;
In
diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3390/molecules181114186