2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

Base Information

Chemical Name:2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid
CAS No.:122408-38-2
Molecular Formula:C₃₆H₅₄N₆*2I*I₂
Molecular Weight:1078.48
Hs Code.:

Synonyms:2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

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Chemical Property of 2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

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Technology Process of 2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

There total 5 articles about 2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 16857-93-5
1,3,5-tris(N-pyrrolidinyl)benzene

: 122408-38-2
2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

Guidance literature:: With iodine; In diethyl ether; dichloromethane; at -40 ℃;

Reference yield:

: 70746-80-4
1-Brom-2,4,6-tris(1-pyrrolidinyl)cyclohexadienylium-bromid

: 122408-38-2
2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / methanol / 0.05 h / Ambient temperature

2: 1.) NaBr, 2.) sodium methylate / 1.) methanol, 1h, room temperature, 2.) methanol, room temperature, 10 min

3: 98 percent / I₂ / CH₂Cl₂; diethyl ether / -40 °C

With iodine; sodium methylate; sodium bromide; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 122408-35-9
1-Iod-2,4,6-tris(1-pyrrolidinyl)cyclohexadienylium-iodid

: 122408-38-2
2,2',4,4',6,6'-Hexakis(1-pyrrolidinyl)-1,1'-bi(cyclohexadienyl)-diium-tetraiodid

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / AgClO₄ / CH₂Cl₂; acetonitrile / 0.5 h / -70 °C

2: 7.5 percent / sodium methylate / methanol / 0.5 h / -40 °C

3: 98 percent / I₂ / CH₂Cl₂; diethyl ether / -40 °C

With iodine; sodium methylate; silver perchlorate; In methanol; diethyl ether; dichloromethane; acetonitrile;