N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

Base Information

Chemical Name:N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide
CAS No.:1616708-00-9
Molecular Formula:C₂₂H₂₆ClN₅O₅
Molecular Weight:475.932
Hs Code.:

Synonyms:N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

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Chemical Property of N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

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Technology Process of N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

There total 6 articles about N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20781-20-8
2,4-Dimethoxybenzylamine

: 1616707-99-3
N'-(2,8-dichloroquinazolin-4-yl)-3,3-dimethoxypropanehydrazide

: 1616708-00-9
N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 80 ℃;

Reference yield:

: 62484-22-4
8-chloroquinazoline-2,4-diol

: 1616708-00-9
N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate; N,N-dimethyl-aniline / 16 h / 140 °C

2: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 2 h / 40 °C

3: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 80 °C

With N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1,4-dioxane;

Reference yield:

: 6388-47-2
2-amino-3-chlorobenzoic acid

: 1616708-00-9
N’-(8-chloro-2-(2,4-dimethoxybenzylamino)quinazolin-4-yl)-3,3-dimethoxypropanehydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 2 h / 200 °C

2: trichlorophosphate; N,N-dimethyl-aniline / 16 h / 140 °C

3: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 2 h / 40 °C

4: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 80 °C

With N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1,4-dioxane;