benzaldehyde azine-3,3'-disulfonyl chloride

Base Information

• Chemical Name: benzaldehyde azine-3,3'-disulfonyl chloride
• CAS No.: 134898-18-3
• Molecular Formula: C₁₄H₁₀Cl₂N₂O₄S₂
• Molecular Weight: 405.282
• Mol file: 134898-18-3.mol

Synonyms:benzaldehyde azine-3,3'-disulfonyl chloride

Chemical Property of benzaldehyde azine-3,3'-disulfonyl chloride

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of benzaldehyde azine-3,3'-disulfonyl chloride

There total 2 articles about benzaldehyde azine-3,3'-disulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

benzaldehyde benzylidenehydrazone (28867-76-7) → benzaldehyde azine-3,3'-disulfonyl chloride (134898-18-3)

Guidance literature:

With chlorosulfonic acid; 1) 120 deg C, 4h, 2) SOCl₂, 2h, RT;

Reference yield: 68.0%

1,2-di(benzylidene)hydrazine (588-68-1) → benzaldehyde azine-3,3'-disulfonyl chloride (134898-18-3)

Guidance literature:

With chlorosulfonic acid;

DOI:10.1080/10426500601142155

Reference yield: 93.0%

benzaldehyde azine-3,3'-disulfonyl chloride (134898-18-3) → C16H20N6O6S2

Guidance literature:

With hydrazine hydrate; In methanol; for 3h; Ambient temperature;

upstream raw materials:

benzaldehyde benzylidenehydrazone

1,2-di(benzylidene)hydrazine

Downstream raw materials:

C₁₄H₁₆N₆O₄S₂

N,N'-Bis-[1-[3-(3,5-dimethyl-morpholine-4-sulfonyl)-phenyl]-meth-(E)-ylidene]-hydrazine

C₂₀H₂₂N₄O₈S₂

C₂₆H₃₄N₄O₈S₂