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4-heptylphenylboronic acid pinacol ester

Base Information Edit
  • Chemical Name:4-heptylphenylboronic acid pinacol ester
  • CAS No.:1359844-04-4
  • Molecular Formula:C19H31BO2
  • Molecular Weight:302.265
  • Hs Code.:
  • Mol file:1359844-04-4.mol
4-heptylphenylboronic acid pinacol ester

Synonyms:4-heptylphenylboronic acid pinacol ester

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Chemical Property of 4-heptylphenylboronic acid pinacol ester Edit
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Technology Process of 4-heptylphenylboronic acid pinacol ester

There total 4 articles about 4-heptylphenylboronic acid pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine; In 1,4-dioxane; at 80 ℃;
DOI:10.1016/j.bmcl.2011.12.043
Guidance literature:
1-bromo-4-heptylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 1h;
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at 20 ℃;
Guidance literature:
Multi-step reaction with 4 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; palladium diacetate / toluene
2: palladium on activated charcoal; hydrogen / ethanol
3: hydrogenchloride; sodium nitrite / water / Cooling with ice
4: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; potassium phosphate monohydrate; palladium on activated charcoal; hydrogen; palladium diacetate; triethylamine; sodium nitrite; In 1,4-dioxane; ethanol; water; toluene; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.12.043
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