(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate
CAS No.:1071476-34-0
Molecular Formula:C₁₉H₂₆F₃N₅O₃
Molecular Weight:429.442
Hs Code.:

Synonyms:(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

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Chemical Property of (S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

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Technology Process of (S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

There total 1 articles about (S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3300-51-4
p-Trifluoromethylbenzylamine

: 333366-32-8
(S)-2-azido-6-((tert-butoxycarbonyl)amino)hexanoic acid

: 1071476-34-0
(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

Guidance literature:: (S)-2-azido-6-((tert-butoxycarbonyl)amino)hexanoic acid; With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

p-Trifluoromethylbenzylamine; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 12h;

Reference yield: 100.0%

: 1071476-34-0
(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

: C₁₄H₁₈F₃N₅O*ClH

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 - 20 ℃; for 2.5h;

Reference yield:

: 1071476-34-0
(S)-tert-butyl 5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylcarbamate

: 1071476-35-1
(S)-4-(5-azido-6-oxo-6-(4-(trifluoromethyl)benzylamino)hexylamino)-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 2.5 h / 0 - 20 °C

2: dmap / 5 h / 20 °C

With hydrogenchloride; dmap; In 1,4-dioxane;