α-(p-tolyl)acrylaldehyde diethyl acetal

Base Information

Chemical Name:α-(p-tolyl)acrylaldehyde diethyl acetal
CAS No.:156020-83-6
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:

Synonyms:α-(p-tolyl)acrylaldehyde diethyl acetal

Suppliers and Price of α-(p-tolyl)acrylaldehyde diethyl acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of α-(p-tolyl)acrylaldehyde diethyl acetal

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

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Technology Process of α-(p-tolyl)acrylaldehyde diethyl acetal

There total 5 articles about α-(p-tolyl)acrylaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 17592-40-4
2-bromo-3,3-diethoxypropene

: 5720-05-8
4-methylphenylboronic acid

: 156020-83-6
α-(p-tolyl)acrylaldehyde diethyl acetal

Guidance literature:: With palladium diacetate; caesium carbonate; XPhos; In 1,4-dioxane; at 40 ℃; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1055/a-1322-3916

Reference yield:

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 156020-83-6
α-(p-tolyl)acrylaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / water; dichloromethane / 2 h / 40 - 60 °C

2: sodium hydroxide / 24 h / Reflux

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In dichloromethane; water;
DOI:10.1039/d1cc04000f

Reference yield:

: 10160-86-8
2,3-dibromo-1,1-diethoxypropane

: 156020-83-6
α-(p-tolyl)acrylaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: palladium diacetate; XPhos; caesium carbonate / 1,4-dioxane / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube

With palladium diacetate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; XPhos; In 1,4-dioxane; dichloromethane; 2: |Suzuki Coupling;
DOI:10.1055/a-1322-3916