2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde

Base Information

Chemical Name:2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde
CAS No.:122801-52-9
Molecular Formula:C₁₁H₁₀Cl₂O
Molecular Weight:229.106
Hs Code.:
DSSTox Substance ID:DTXSID501196091

Synonyms:122801-52-9;2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde;DTXSID501196091

Suppliers and Price of 2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:228.0108703
Heavy Atom Count:14
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2(CC2(Cl)Cl)C=O

Technology Process of 2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde

There total 3 articles about 2,2-Dichloro-1-(4-methylphenyl)cyclopropanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.1%

: 156020-84-7
2,2-dichloro-1-(p-tolyl)cyclopropanecarbaldehyde diethyl acetal

: 122801-52-9
2,2-dichloro-1-(p-tolyl)cyclopropanecarbaldehyde

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 50 ℃; for 6h;
DOI:10.1039/P19940000739

Reference yield:

: C₉H₉ClMg

: 122801-52-9
2,2-dichloro-1-(p-tolyl)cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 38.9 percent / tetrahydrofuran / Ambient temperature

2: 37.3 percent / 18-crown-6 / 1,2-dimethoxy-ethane / 5 h / Heating

3: 22.1 percent / conc. HCl / dioxane / 6 h / 50 °C

With hydrogenchloride; 18-crown-6 ether; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane;
DOI:10.1039/P19940000739

Reference yield:

: 156020-83-6
α-(p-tolyl)acrylaldehyde diethyl acetal

: 122801-52-9
2,2-dichloro-1-(p-tolyl)cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 37.3 percent / 18-crown-6 / 1,2-dimethoxy-ethane / 5 h / Heating

2: 22.1 percent / conc. HCl / dioxane / 6 h / 50 °C

With hydrogenchloride; 18-crown-6 ether; In 1,4-dioxane; 1,2-dimethoxyethane;
DOI:10.1039/P19940000739