3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

Base Information

Chemical Name:3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide
CAS No.:1246960-11-1
Molecular Formula:C₂₇H₄₆N₂O₃Si
Molecular Weight:474.759
Hs Code.:

Synonyms:3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

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Technology Process of 3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

There total 1 articles about 3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.6%

: 1246960-10-0
C₁₂H₂₉NOSi

: 1246959-90-9
3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]benzoic acid

: 1246960-11-1
3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

Guidance literature:: With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 0 - 50 ℃;

Reference yield: 70.3%

: 1246960-11-1
3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide

: (R)-VSN₁₆

Guidance literature:: 3-[(1Z)-6-(dimethylamino)-6-oxohex-1-en-1-yl]-N-(2-triisopropylsilyloxy-1-methyl-ethyl)benzamide; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 18h;

With hydrogenchloride; In tetrahydrofuran; ethyl acetate;