2-methoxy-6-methoxycarbonylphenyl azide

Base Information

Chemical Name:2-methoxy-6-methoxycarbonylphenyl azide
CAS No.:1379607-21-2
Molecular Formula:C₉H₉N₃O₃
Molecular Weight:207.189
Hs Code.:

Synonyms:2-methoxy-6-methoxycarbonylphenyl azide

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Chemical Property of 2-methoxy-6-methoxycarbonylphenyl azide

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Technology Process of 2-methoxy-6-methoxycarbonylphenyl azide

There total 2 articles about 2-methoxy-6-methoxycarbonylphenyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 5121-34-6
methyl 2-amino-3-methoxybenzoate

: 1379607-21-2
2-methoxy-6-methoxycarbonylphenyl azide

Guidance literature:: methyl 2-amino-3-methoxybenzoate; With hydrogenchloride; In tetrahydrofuran; water; Cooling;

With sodium nitrite; In tetrahydrofuran; water; at 0 - 5 ℃;

With sodium azide; In tetrahydrofuran; water; at 5 - 20 ℃;
DOI:10.1021/jp3025705

Reference yield:

: 1379607-21-2
2-methoxy-6-methoxycarbonylphenyl azide

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.333333h; Inert atmosphere;

With sodium azide; sodium acetate; In water; at 0 - 20 ℃; for 1.33333h; Inert atmosphere;