1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

Base Information

Chemical Name:1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide
CAS No.:439117-79-0
Molecular Formula:C₃₇H₄₄ClN₃O₇
Molecular Weight:678.225
Hs Code.:

Synonyms:1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

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Chemical Property of 1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

Chemical Property:

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Technology Process of 1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

There total 3 articles about 1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4-tert-butoxycarbonylphenyl)(hydroxy)phenylacetic acid

: 80029-43-2,123333-53-9
1-hydroxybenzotriazol-hydrate

: 439117-44-9
(S)-tert-butyl 4-chloro-2-((pyrrolidine-2-carboxamido)methyl)benzylcarbamate

: 439117-79-0
1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

Guidance literature:: With 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: ethyl (4-tert-butyloxycarbonylphenyl)(hydroxy)phenylacetate

: 439117-79-0
1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol

2: 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide; acetonitrile

With sodium hydroxide; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; In methanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1603-79-8
phenylglyoxylic acid ethyl ester

: 439117-79-0
1-(2-(4-tert-butyloxycarbonylphenyl)-2-hydroxy-2-phenylethanoyl)-N-(2-tert-butyloxycarbonylaminomethyl-5-chlorobenzyl)-L-prolinamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride / tetrahydrofuran; ethyl acetate

2: sodium hydroxide / methanol

3: 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide; acetonitrile

With sodium hydroxide; ammonium chloride; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;