2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone

Base Information

• Chemical Name: 2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone
• CAS No.: 126681-77-4
• Molecular Formula: C₂₀H₂₀BrNO₂
• Molecular Weight: 386.288
• Mol file: 126681-77-4.mol

Synonyms:2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone

Chemical Property of 2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone

There total 1 articles about 2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

4-bromo-5-phenyl-2,3-dihydrofurandione (126681-83-2) + 1-adamantyl isocyanate (4411-25-0) → 2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone (126681-77-4)

Guidance literature:

In xylene; for 1h; Heating;

DOI:10.1007/BF00764713

Reference yield: 40.0%

2-1-adamantyl)imino>-4-bromo-5-phenyl-2,3-dihydro-3-furanone (126681-77-4) → 1-adamantylamine hydrobromide (88545-10-2) + 1-chloroacetophenone (532-27-4,108321-66-0,164322-25-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 3h; Product distribution; other subst. furanone;

DOI:10.1007/BF00764713

upstream raw materials:

4-bromo-5-phenyl-2,3-dihydrofurandione

1-adamantyl isocyanate

Downstream raw materials:

1-adamantylamine hydrobromide

1-chloroacetophenone