N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide

Base Information

• Chemical Name: N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide
• CAS No.: 1432625-91-6
• Molecular Formula: C₄₂H₄₆Br₂N₄O₄
• Molecular Weight: 830.66
• Mol file: 1432625-91-6.mol

Synonyms:N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide

Chemical Property of N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide

There total 3 articles about N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,3,6,7-tetrabromonaphthalene-1,8,4,5-tetracarboxylic acid N,N-dioctyldiimide (954374-43-7) + aniline (62-53-3) → N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-91-6)

Guidance literature:

With tetra-n-butylammoniumfluoride trihydrate; In dichloromethane; at 20 ℃; for 2h; Time; Concentration; regioselective reaction;

DOI:10.1021/jo400320a

Reference yield: 29.0%

2,3,6,7-tetrabromonaphthalene-1,8,4,5-tetracarboxylic acid N,N-dioctyldiimide (954374-43-7) + aniline (62-53-3) → N,N′-di-(n-octyl)-2,3,6-tribromo-7-phenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-84-7) + N,N′-di-(n-octyl)-2,7-dibromo-3,6-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-85-8) + N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-91-6) + N,N′-di-(n-octyl)-2,6-dibromo-3,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-92-7)

Guidance literature:

In N,N-dimethyl-formamide; at 135 ℃; for 1h; Time; Solvent; Reagent/catalyst; regioselective reaction;

DOI:10.1021/jo400320a

Reference yield:

2,3,6,7-tetrabromonaphthalene-1,8,4,5-tetracarboxylic acid N,N-dioctyldiimide (954374-43-7) + aniline (62-53-3) → N,N′-di-(n-octyl)-2,7-dibromo-3,6-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-85-8) + N,N′-di-(n-octyl)-2,3-dibromo-6,7-diphenylamino-1,4,5,8-naphthalenetetracarboxylic acid diimide (1432625-91-6)

Guidance literature:

In N,N-dimethyl-formamide; at 65 ℃; for 2h; Time; Solvent; regioselective reaction;

DOI:10.1021/jo400320a

upstream raw materials:

2,3,6,7-tetrabromonaphthalene-1,8,4,5-tetracarboxylic acid N,N-dioctyldiimide

aniline