2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester
CAS No.:1365553-86-1
Molecular Formula:C₂₇H₃₉NO₅S
Molecular Weight:489.676
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Suppliers and Price of 2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

There total 5 articles about 2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1365555-24-3
3-methylpent-1-en-4-yn-3-yl pivalate

: 1365556-03-1
C₁₆H₂₃NO₃S

: 1365553-86-1
2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Guidance literature:: With Wilkinson's catalyst; In chloroform; at 65 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja2109097

Reference yield:

: C₁₇H₂₃NO₄S

: 1365553-86-1
2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

2: Wilkinson's catalyst / chloroform / 65 °C / Inert atmosphere

With Wilkinson's catalyst; lithium aluminium tetrahydride; In tetrahydrofuran; chloroform;
DOI:10.1021/ja2109097

Reference yield:

: 68305-83-9,51220-84-9
N-Tosyl-DL-leucin-methylester

: 1365553-86-1
2,2-dimethyl-propionic acid 4-[(1-hydroxymethyl-3-methyl-butyl)-(toluene-4-sulfonyl)-amino]-methyl-7-methyl-cyclohepta-1,3,6-trienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

3: Wilkinson's catalyst / chloroform / 65 °C / Inert atmosphere

With Wilkinson's catalyst; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja2109097