[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

Base Information

Chemical Name:[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid
CAS No.:1341126-89-3
Molecular Formula:C₁₇H₁₈N₂O₅S
Molecular Weight:362.406
Hs Code.:

Synonyms:[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

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Chemical Property of [5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

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Technology Process of [5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

There total 4 articles about [5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1341126-95-1
methyl [5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetate

: 1341126-89-3
[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

Guidance literature:: methyl [5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetate; With lithium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 1h;

pH=1; Acidic aq. solution;
DOI:10.1016/j.bmc.2011.08.054

Reference yield:

: 1341126-59-7
2-(3-phenoxybenzyl)-1,2,5-thiadiazolidine 1,1-dioxide

: 1341126-89-3
[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 20 °C

2.1: lithium hydroxide / 1,4-dioxane; water / 1 h / 20 °C

2.2: pH 1 / Acidic aq. solution

With sodium hydride; lithium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.054

Reference yield:

: N-(3-phenoxybenzyl)ethane-1,2-diamine

: 1341126-89-3
[5-(3-phenoxybenzyl)-1,1-dioxido-1,2,5-thiadiazolidin-2-yl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; SULFAMIDE / 16 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 20 °C

3.1: lithium hydroxide / 1,4-dioxane; water / 1 h / 20 °C

3.2: pH 1 / Acidic aq. solution

With pyridine; sodium hydride; SULFAMIDE; lithium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.054