C₁₆H₂₈O₄

Base Information

• Chemical Name: C₁₆H₂₈O₄
• CAS No.: 945426-69-7
• Molecular Formula: C₁₆H₂₈O₄
• Molecular Weight: 284.396
• Mol file: 945426-69-7.mol

Synonyms:C₁₆H₂₈O₄

Chemical Property of C₁₆H₂₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₈O₄

There total 7 articles about C₁₆H₂₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H26O3 (945426-67-5) + acetyl chloride (75-36-5) → C16H28O4 (945426-69-7)

Guidance literature:

With pyridine; In diethyl ether; at 0 - 20 ℃;

DOI:10.1080/00397910701196546

Reference yield:

4-(2,6,6-trimethyl-2-cyclohexen-1-ylidene)-2-methoxybutane (945426-65-3) → C16H28O4 (945426-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: anhydrous sodium carbonate; m-chloroperbenzoic acid / CH₂Cl₂ / 8 h / 20 °C

1.2: 220 mg / sulfuric acid / H₂O; diethyl ether / 6 h / 20 °C

2.1: pyridine / diethyl ether / 0 - 20 °C

With pyridine; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

DOI:10.1080/00397910701196546

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) → C16H28O4 (945426-69-7)

Guidance literature:

Multi-step reaction with 4 steps

1.1: isopropenyl acetate; p-toluenesulfonic acid monohydrate / 24 h / Heating

1.2: NaBH₄ / aq. ethanol / 1.5 h / Heating

2.1: 96 percent / sodium hydride / dimethylformamide / 0 - 20 °C

3.1: anhydrous sodium carbonate; m-chloroperbenzoic acid / CH₂Cl₂ / 8 h / 20 °C

3.2: 220 mg / sulfuric acid / H₂O; diethyl ether / 6 h / 20 °C

4.1: pyridine / diethyl ether / 0 - 20 °C

With pyridine; Isopropenyl acetate; sodium hydride; sodium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1080/00397910701196546

upstream raw materials:

C₁₄H₂₆O₃

acetyl chloride

C₁₄H₂₄O₃

4-(2,6,6-trimethyl-2-cyclohexen-1-ylidene)-2-methoxybutane

Downstream raw materials:

C₁₆H₂₆O₄

(E)-3-(but-2-enoyl)-2,4,4-trimethylcyclohex-2-en-1-yl acetate

Damascenon